MIneralogy and thin sections

About Mineralogy and Thin sections

The purpose of preparation of rocks, minerals, ceramic and biological specimens is most often:

  • Classification of rocks
  • Identification and mapping of minerals e.g. dating or exploration
  • Analysis e.g. major and trace elements, textural studies or isotopic composition
  • Studies of fluid inclusions
  • Studies of micro fossils
  • Studies of rock fabrics e.g. porosity and permeability
  • Studies of texture and age of bones/teeth

Specimen Types

Specimen types can be split into four groups:

  1. Thin Sections (30µm) (+ cover glass) - for examination in transmitted light or electron microscope/probe
  2. Polished Thin sections - for examination in transmitted/reflected light or electron microscope/probe
  3. Thick Sections (~100µm) - for examination in reflected light or electron microscope/probe
  4. Polished blocks/mounts - for examination in reflected light or electron microscope/probe

Specimen types 1)+2)+3) all have “special requirements” from a materialographic point of view. Differences between the three types are characterised by surface finish and specimen thickness.

Specimen type 4 is a more conventional materialographic specimen in terms of requirements.

The same mineralogical material will have similar preparation methods across the four different specimen types, as the material characteristics are decisive for all the preparation steps.

How to do mineralogical and thin section preparation

How to do Thin Sections

The production of thin sections is a multistep process which requires highly specialised equipment.
Combining the equipment, the consumables, the work process and method depends on the type of specimen. A general workflow is described. Mineralogical specimens will be described in more details below.

  1. Sampling from larger section
  2. Cutting of a specimen to e.g. 20x30x8 mm
  3. Grinding or lapping of the specimen to complete planeness
  4. Grinding of glass slide to complete planeness and a well defined thickness
  5. Cementing the specimen to glass slide using vacuum impregnation
  6. Cutting off surplus specimen material to a thickness of 0.5-2 mm.
  7. Grinding of thin sections to a thickness of 80 µm
  8. Grinding or lapping of thin section to final thickness of section + resin e.g. 30 µm.
  9. Polishing of thin sections removing approximately 10 µm.

How to do Polished blocks/mounts

The preparation of polished blocks/mounts is similar to the preparation of other materials. The procedures related to cutting in special specimen sizes, gluing to glass slides, etc. is excluded from the workflow. These types of specimens follow a conventional 4-step process where parameters and consumables in each step are carefully selected in accordance to the type of material.
Cutting to manage specimen

1. Cutting to manageable specimen size and geometry

Mounting if required

2. Mounting if required for reaching manageable geometry or for specimen protection.

Grinding lapping

3. Grinding/lapping to remove surface damage, reach planeness and prepare surface for polishing.

Polishing to reveal true structure

4. Polishing to reveal true structure and achieve surface reflectiveness.

Mineralogical Specimen Preparation

Mineralogical specimens are often hard, brittle, porous and inhomogeneous. They can contain extremely hard and soft phases that require accessories specially developed for these materials

Struers Mineralogram - “Mineralogy Methods Cube”
The Methods Cube covers standard thin section preparation methods for a wide range of minerals. It was developed in collaboration with GEUS (The Geological Survey of Denmark and Greenland).

Visualization of our cube:
  • Along with GEUS it was determined that a cube would provide the best representation of mineral properties. The cube is divided into three 2-dimensional squares to make it easy to work with and understand.
  • The hardness of rock is a term that can be difficult to handle because rocks are a kind of “composite” (and a mix of minerals with potentially different hardness). Important rock parameters, both alone and in combination with others, are internal structure (column equality, slate-like cleavage), and the extent to which the rock has been subject to pressure, and/or (partially) converted by various liquids or molten rock.
  • A rock may encounter isotropic properties that must be assessed for each specimen by looking at the mineral along with the general structure of the rock, and considering whether there are other conditions that may affect the hardness.
Mohs Hardness table

Hardness

Hardness is defined by the hardest mineral that makes up at least 15% of the rock.

The cube will be divided into three 2D charts, representing 3 levels of hardness (Mohs)
- Soft (1-3)
- Medium (4-6)
- Hard (7-10)

The homogeneity / heterogeneity of a rock is not determined by smaller or larger mineral content. It is related to the rock face "texture" including the internally related grain size of the minerals and its immediate appearance. To put it simply, one can say that a rock can be characterised as homogeneous if it appears structurally and compositionally uniform in all directions (uniform pattern).

Consolidation

Consolidation

Make something physically stronger and more solid
Consolidated: sticking well together – so the material becomes stronger or more solid/massive

Interlocked grains, fracture/porous free
Unconsolidated: ’loose’ – porous - breaks easily – poorly cemented grains etc

Homogeneity

Homogeneity

Homogeneity and heterogeneity are concepts relating to the uniformity in a material
Homogeneous material is uniform in composition or character – similar properties
Heterogeneous material is distinctly non-uniform in these qualities

Sample Materials

To demonstrate our idea, we have displayed 10 materials from the list below in sections of the Mineralogram. Three preparation methods are specified to cover the span of materials in the cube. Also a method for reactive or water sensitive materials is given.

How to do mineralogical and thin section preparation

Sample materials Mineralogram

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